GNE-7915_LCMS_12731_MedChemExpress

File ..M32\1\DATA\20170221\CPK\CPK2017-221-12731.D Tgt Mass (EZX): 443.40 Injection Date : 21 Feb 17 3:40 pm +0800 Seq. Line : 0 Sample Name : CPK2017-221-12731 Location : P2-D-06 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M

Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M

Catalog No: HY-18163 Batch#12731 Easy-Access Method: '1-POS-3MIN' 443.40 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C

min*

0.5

1

1.5

2 2.5mAU 0

200400

600*DAD1 B, Sig=214,4 Ref=off 1.170

1.2531.3201.444

1.727

1.947

min*

0.51

1.5

2 2.5mAU 0

200400

*DAD1 C, Sig=254,4 Ref=off 1.321

1.537

1.727

1.8791.910

min

0.51 1.5

2

2.5

100000

200000300000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

1.736

min

0.5

1

1.5

2

2.5

50000

100000150000200000 Ion 444.4, MSD1 444.4,Target Mass 443.4 +H Positive, EIC=444.1:445.1

1.734

Integration Results for DAD1 B, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.17 0.03 1.66 1.09 0.10 ND 1.25 0.02 3.29 2.63 0.20 ND 1.32 0.03 5.68 3.09 0.35 294 1.44 0.03 6.44 0.30 0.40 242 1.73 0.03 1590.26 817.22 98.77 444 1.95 0.03 2.75 1.66 0.17 338

Integration Results for DAD1 C, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.32 0.04 7.68 3.13 0.66 ND 1.54 0.03 2.31 1.25 0.20 ND 1.73 0.03 1147.91 589.77 98.88 444 1.88 0.04 1.24 0.52 0.11 444 1.91 0.04 1.81 0.30 0.16 338

Ret. Time: 1.74 <<<< POSITIVE SPECTRA >>>>

m/z

200

300

400

500

600

700

800

900

10000

200003000040000

50000600007000080000 ES-API Positive

909.2

445.2 444.1