氧化亚铜 XRD测量数据

寻峰报表(5个峰标,最大峰噪比=11.8)

[07125-20.mdi] DX-2700 CSC 35kV/25mA Slit:1deg&1deg&.2mm Monochromator: ON Ts-Td 寻峰: 9(点)/四次项筛选,阈值=5.5,下限=0.1%,背景=3/1.0,峰标=峰顶法

2θd(埃) 背景峰高峰高% 面积面积% 半峰宽晶粒(埃)

36.7420 2.4441 51.3 599.7 100.0 1336.3 100.0 0.284 370

42.6642 2.1175 72.8 215.2 35.9 330.5 24.7 0.184 735

61.7839 1.5003 72.0 208.0 34.7 399.7 29.9 0.245 504

73.9729 1.2804 66.4 116.6 19.5 310.7 23.3 0.340 349

77.9345 1.2249 60.2 31.8 5.3 39.1 2.9 0.150 >1000

PDF#04-003-6433(RDB):质标=定胞(I);d=计算值;I=计算值

Cuprite, syn(Copper Oxide)

Cu2 O

射线=CuKa1 波长=1.5406 滤波法=

校准= 2θ=29.7037-140.7057 I/Ic(K值)=8.07

文献: Pinsker Z.G., Imamov R.M.

Sov. Phys. Crystallogr. (Engl. Transl.), v9 p334(1964)

立方晶系-(未知),Pn-3m(224) Z=2

晶胞: 4.25x4.25x4.25 <90.0x90.0x90.0> P.S=cP6.00

密度(计算)=6.19 密度(测量)= 分子量=143.09 体积=76.77 F(20)=999.9(0.0002,20/0) 文献: 出处同上

强峰线: 2.45/X 2.13/3 1.50/3 1.28/2 3.01/1

ANX: A2X.

LPF Collection Code: 457773.

Sample Preparation: Compound Preparation: vaporization of Cu wire under vacuum followed by condensation of freshly cleaved surfaces of rocksalt.

Sample annealed at 433-443 K.

Minor Warning: Magnitude of e.s.d.

on cell dimension is >1000 ppm.

Unit Cell Data Source: Electron diffraction.

2θd(埃) I(f) ( h k l) θ1/(2d) 2π/d n^2

29.7037 3.0052 5.4 ( 1 1 0) 14.8519 0.1664 2.0908 2

36.5921 2.4537 100.0 ( 1 1 1) 18.2960 0.2038 2.5607 3

42.5066 2.1250 34.3 ( 2 0 0) 21.2533 0.2353 2.9568 4

52.7135 1.7351 1.1 ( 2 1 1) 26.3567 0.2882 3.6213 6

61.6799 1.5026 25.4 ( 2 2 0) 30.8399 0.3328 4.1815 8

65.8767 1.4167 0.1 ( 2 2 1) 32.9384 0.3529 4.4352 9

69.9402 1.3440 0.3 ( 3 1 0) 34.9701 0.3720 4.6751 10

73.9012 1.2814 18.4 ( 3 1 1) 36.9506 0.3902 4.9033 11

77.7839 1.2269 3.9 ( 2 2 2) 38.8920 0.4075 5.1213 12

85.4001 1.1359 0.2 ( 3 2 1) 42.7000 0.4402 5.5317 14 92.9350 1.0625 2.1 ( 4 0 0) 46.4675 0.4706 5.9136 16 96.7129 1.0308 0.1 ( 3 2 2) 48.3565 0.4851 6.0956 17 100.5220 1.0017 0.1 ( 4 1 1) 50.2610 0.4991 6.2723 18 104.3771 0.9750 4.7 ( 3 3 1) 52.1885 0.5128 6.4442 19 108.3006 0.9503 3.4 ( 4 2 0) 54.1503 0.5261 6.6116 20 112.3153 0.9274 0.1 ( 4 2 1) 56.1576 0.5391 6.7749 21 116.4491 0.9061 0.1 ( 3 3 2) 58.2246 0.5518 6.9343 22 125.2259 0.8675 3.7 ( 4 2 2) 62.6130 0.5764 7.2426 24 135.0888 0.8335 0.1 ( 4 3 1) 67.5444 0.5999 7.5384 26 140.7057 0.8179 3.4 ( 5 1 1) 70.3528 0.6113 7.6820 27

100

0100200300400

500600

700峰高

2θ

0.04

0.06

0.08

0.10

0.12

0.140.160.180.20

6810121416

20平衡吸

附量吸附平衡浓度C

100

200

300

400

40000

42000440004600048000500005200054000

560005800060000表

面张力乙醇浓度C

200

400

600

800

1000

1200

1400

吸

附量乙醇浓度C